2,4-Dimethoxybenzoic acid → 5-Bromo-2,4-dimethoxybenzoic acid

Participants

Reaction Steps

To a solution of 2,4-dimethoxybenzoic acid (4.0 g, 0.022 mol) in chloroform (60 ml) was added bromine (1.13 ml, 0.022 mol) in chloroform (20 ml) dropwise. After stirring overnight at room temperature the precipitate was filtered off and dried to afford the title compound as a white solid (2.87 g).

Provenance & Evidence