HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 22597833, compound → HCID 22597863, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 22597833 | HCID 22597833 | — |
| Reactant | HCID 178418546 | HCID 178418546 | — |
| Solvent | N-methyl-2-pyrrolidone | HCID 13387 | — |
| Product | HCID 22597863 | HCID 22597863 | 40.3% |
Reaction Steps
Ethyl 2-ethoxy-4-iso-propyl-5-bromobenzoate (12 g, 3.8 mmol) was treated with copper (I) cyanide (682 mg, 7.6 mmol) in N-methyl-2-pyrrolidinone (40 ml) as described in Procedure 5 to give the title compound as an oil (400 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492378B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a5e16f1f3b8c4324a4f43d7ea9e14a7e |
| Source note | uspto-grants-2002_12 |