HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Thiopheneboronic acid → (1H-Indol-5-yl)-(2-thiophen-2-yl-thieno[3,2-b]pyridin-7-yl)-amine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Thiopheneboronic acid | HCID 2733960 | — |
| Reactant | (2-bromo-thieno[3,2-b]pyridin-7-yl)-(1H-indol-5-yl)-amine | HCID 18382766 | — |
| Product | (1H-Indol-5-yl)-(2-thiophen-2-yl-thieno[3,2-b]pyridin-7-yl)-amine | HCID 9884654 | — |
Reaction Steps
The title compound was prepared from thiophene-2-boronic acid and (2-bromo-thieno[3,2-b]pyridin-7-yl)-(1H-indol-5-yl)-amine by a procedure analogous to example 17. 1H NMR (400 MHz, DMSO) d 11.1 (s, 2H), 8.27 (d, 1H), 7.73 (s, 1H), 7.48 (m, 5H), 7.19 (m, 1), 7.03 (d, 1H), 6.50 (s, 1H); LC-MS: 348 (MH+); HPLC RT: 5.11 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492383B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-b3688f23300a4528bcf689bfbe199a33 |
| Source note | uspto-grants-2002_12 |