HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 2757862, compound → HCID 18382865, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 2757862 | HCID 2757862 | — |
| Reactant | HCID 4764078 | HCID 4764078 | — |
| Product | HCID 18382865 | HCID 18382865 | 21% |
Reaction Steps
Utilizing a procedure analogous to that described in Example 61, the title compound was prepared in 21% yield from N-m-Tolyl-benzene-1,4-diamine (230 mg, 1.16 mmol) and 4-chloro-6-phenyl-thieno[3,2-d]pyrimidine 250 mg, 1.16 mmol). RP18-HPLC RT: 7.432 minutes; APl MS: 409.1 (M+1); MP: 170-171° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492383B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-11b8dc0979e2434dab88ba82aaf70cb2 |
| Source note | uspto-grants-2002_12 |