5-Bromo-2-chlorobenzoic acid → 5-bromo-2-chloro-N-(tricyclo[3.3.1.13,7]dec-1-ylmethyl)benzamide

Participants

Reaction Steps

Prepared as in Example 1a from 5-bromo-2-chlorobenzoic acid (7.17 g), oxalyl chloride (5.3 ml), dichloromethane (150 ml), dimethylformamide (0.05 ml), diisopropylethylamine (6 ml) and adamantylmethylamine (5 ml) to give the subtitle compound as white colourless needles (7.3 g).

Provenance & Evidence