Ethyl Acetate → HCID 12082818, compound

Participants

Reaction Steps

To a solution of the alcohol prepared in Example 131, Step 3 (1.1 g, 3.3 mmol) in ethyl acetate (20 mL) was added MnO2 (5 g, 60 mmol) and the mixture stirred at room temperature overnight. The mixture was Filtered through Celite and the solution was concentrated to provide the crude aldehyde.

Provenance & Evidence