HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 18386460, compound → HCID 23664898, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 18386460 | HCID 18386460 | — |
| Reactant | Butyllithium | HCID 178418339 | — |
| Solvent | Pentane | HCID 8003 | — |
| Product | HCID 23664898 | HCID 23664898 | — |
Reaction Steps
4-(2-methylphenyl)-2-isopropylindene (6.6 g, 26.5 mmol) was dissolved in 80 mL of pentane. To this solution was added 10.6 mL of n-BuLi (2.5M in hexane) and the reaction was allowed to stir 4 hours at room temperature. A white solid precipitates from solution and was collected by frit filtration and washed with additional pentane. Yield was 5.8 g (88%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06492465B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-e9de95255b2a4415874f41a4dd41f6f8 |
| Source note | uspto-grants-2002_12 |