4-Pentenal → HCID 69463025, compound

HRID 2298553Notes

Reaction equation

HRID 2298553 reaction equation
[C:1]([N:5]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[O:7][C:6]1=[O:14])(=[O:4])[CH2:2][CH3:3].[CH:15](=[O:20])[CH2:16][CH2:17][CH:18]=[CH2:19]>>[CH3:3][C@H:2]([C@@H:15]([OH:20])[CH2:16][CH2:17][CH:18]=[CH2:19])[C:1]([N:5]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[O:7][C:6]1=[O:14])=[O:4]

Participants

3

Reactant 2

HCID 164184-PentenalHCID 8437913-Propionyl-2-benzoxazolinone

Product 1

HCID 69463025HCID 69463025, compound

Procedure

Was prepared according to the method of paragraph C by reaction of N-propionyl-2-benzoxazolinone with 4-pentenal. 13C-NMR (CDCl3, 100 MHz): δ 176.28, 151.07, 142.20, 137.96, 127.75, 125.50, 124.89, 116.26, 115.19, 109.89, 70.93, 43.76, 33.12, 30.16, 10.21.

Workup

  1. customWas prepared

Sources & evidence

ORD record
ord-e2c3801f13714a19a0240fd4c160d50d
Source dataset
uspto-grants-2002_12
Patent number
US06492562B1

Reaction notes

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