Benzenepropanal → HCID 69465361, compound

HRID 2298556Notes

Reaction equation

HRID 2298556 reaction equation
[C:1]([N:5]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[O:7][C:6]1=[O:14])(=[O:4])[CH2:2][CH3:3].[C:15]1([CH2:21][CH2:22][CH:23]=[O:24])[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[CH3:3][C@H:2]([C@@H:23]([OH:24])[CH2:22][CH2:21][C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[C:1]([N:5]1[C:9]2[CH:10]=[CH:11][CH:12]=[CH:13][C:8]=2[O:7][C:6]1=[O:14])=[O:4]

Participants

3

Reactant 2

HCID 7707BenzenepropanalHCID 8437913-Propionyl-2-benzoxazolinone

Product 1

HCID 69465361HCID 69465361, compound

Procedure

Prepared according to the method of paragraph C by reaction of N-propionyl-2-benzoxazolinone with 3-phenylpropanal. 1H-NMR (CDCl3, 400 MHz): δ 8.06 (m, 1H); 7.25 (m, 8H); 4.11 (dt, 1H, J=4,7); 3.96 (dq, 1H, J=3,7); 2.91 (m, 1H); 2.70 (m, 1H); 1.95 (m, 1H); 1.81 (m, 1H); 1.34 (t, 3H, J=7).

Workup

  1. customPrepared

Sources & evidence

ORD record
ord-6b17304920744fe091ae89e95a21be61
Source dataset
uspto-grants-2002_12
Patent number
US06492562B1

Reaction notes

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