Ammonium formate → HCID 11444889, compound

Participants

Reaction Conditions

Reaction Steps

To 10% palladium on carbon (1.6 g) under nitrogen was added a solution of Intermediate 5 (1.67 g, 2.38 mM) in ethanol (50 ml) followed by ammonium formate (0.72 g, 11.9 mM). The mixture was heated to 50° C. for 4 h., filtered through a pad of Harborlite®. The filtrate was evaporated under reduced pressure to yield the title compound as a pale yellow solid (1.45 g).

Provenance & Evidence