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Benzylamine → Ethyl 3-(benzylamino)butanoate
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Benzylamine | HCID 7504 | — |
| 反応物 | Ethyl trans-crotonate | HCID 429065 | — |
| 生成物 | Ethyl 3-(benzylamino)butanoate | HCID 236384 | 69% |
反応手順
A solution of ethyl crotonate (5.0 ml, 40 mmol) and benzyl amine (4.8 ml, 44 mmol) was heated to 100° C. for 18 hs. The reaction was allowed to cool and the product was distilled at 90° C. at 200 mtorr pressure to give the ethyl 3-(benzylamino)butanoate (6.1 g, 69%) as a clear oil, MS (M+H)+=222.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US06495565B2 |
| 出典データセット | uspto-grants-2002_12 |
| ORD ID | ord-848a448f0af148e48bd99e9eb0f9003f |
| 出典メモ | uspto-grants-2002_12 |