2-(3,4-Dichloro-phenylamino)-propionic Acid → HCID 18341188, compound

HRID 2299536Notes

Reaction equation

HRID 2299536 reaction equation
[CH3:1][N:2]([CH3:10])[C:3](=[O:9])[C@H:4]([CH:6]([CH3:8])[CH3:7])[NH2:5].[Cl:11][C:12]1[CH:13]=[C:14]([NH:19][CH:20]([C:22](O)=[O:23])[CH3:21])[CH:15]=[CH:16][C:17]=1[Cl:18]>>[CH3:1][N:2]([CH3:10])[C:3](=[O:9])[C@H:4]([CH:6]([CH3:8])[CH3:7])[NH:5][C:22](=[O:23])[CH:20]([CH3:21])[NH:19][C:14]1[CH:15]=[CH:16][C:17]([Cl:18])=[C:12]([Cl:11])[CH:13]=1

Participants

3

Reactant 2

HCID 69164262-(3,4-Dichloro-phenylamino)-propionic AcidHCID 14963845HCID 14963845, compound

Product 1

HCID 18341188HCID 18341188, compound

Procedure

Following General Procedure D and using valine N,N-dimethyl amide (from Example D above) and N-(3,4-dichlorophenyl)-D,L-alanine (from Example A above), the title compound was prepared as a solid (mp=145-160° C.).

Sources & evidence

ORD record
ord-c953250c0433453d9fa4e3ebbfe772ba
Source dataset
uspto-grants-2002_12
Patent number
US06495693B2

Reaction notes

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