2-(3,4-Dichloro-phenylamino)-propionic Acid → HCID 18341195, compound

HRID 2299537Notes

Reaction equation

HRID 2299537 reaction equation
[CH3:1][NH:2][C:3](=[O:9])[C@H:4]([CH:6]([CH3:8])[CH3:7])[NH2:5].[Cl:10][C:11]1[CH:12]=[C:13]([NH:18][CH:19]([C:21](O)=[O:22])[CH3:20])[CH:14]=[CH:15][C:16]=1[Cl:17]>>[CH3:1][NH:2][C:3](=[O:9])[C@H:4]([CH:6]([CH3:8])[CH3:7])[NH:5][C:21](=[O:22])[CH:19]([CH3:20])[NH:18][C:13]1[CH:14]=[CH:15][C:16]([Cl:17])=[C:11]([Cl:10])[CH:12]=1

Participants

3

Reactant 2

HCID 69164262-(3,4-Dichloro-phenylamino)-propionic AcidHCID 11423608N-Methyl-L-valinamide

Product 1

HCID 18341195HCID 18341195, compound

Procedure

Following General Procedure D and using L-valine N-methyl amide (from Example E above) and N-(3,4-dichlorophenyl)-D,L-alanine (from Example A above), the title compound was prepared as a solid (mp=145-160° C.).

Sources & evidence

ORD record
ord-199cb549810946b19edba2d8009f50d8
Source dataset
uspto-grants-2002_12
Patent number
US06495693B2

Reaction notes

Loading…