HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-Alanine → HCID 18341175, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-Alanine | HCID 5950 | — |
| Reactant | 2-(3,4-Dichloro-phenylamino)-propionic Acid | HCID 6916426 | — |
| Reactant | 3,5-Diiodotyrosine methyl ester hydrochloride, L- | HCID 56777166 | — |
| Product | HCID 18341175 | HCID 18341175 | — |
Reaction Steps
Following General Procedure D and using 3,5-diiodo-L-tyrosine methyl ester hydrochloride (Bachem) and N-(3,4-dichlorophenyl)-D,L-alanine (from Example A above), the title compound was prepared as a mixture of stereoisomers about alanine. The reaction was monitored by tic (Rf=0.29 in 10% MeOH/CH2Cl2) and purification was by flash chromatography (10% methanol/methylene chloride).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495693B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-19610d83877f4fa1a31257cb5d88628c |
| Source note | uspto-grants-2002_12 |