HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexanoic Acid → HCID 21969911, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexanoic Acid | HCID 8892 | — |
| Reactant | HCID 54093670 | HCID 54093670 | — |
| Product | HCID 21969911 | HCID 21969911 | — |
Reaction Steps
Following General Procedure D and using N-[N-(3,4-dichlorophenyl)-D,L-alanyl]-L-lysine methyl ester (from Example 21 above) and hexanoic acid (Aldrich), the title compound was prepared. The reaction was monitored by tlc (Rf=0.38 in 60% CH2CH2/10% hexanes/27% EtOAc/3% MeOH) and purification was by flash chromatography using 60% CH2CH2/10% hexanes/ 27% EtOAc/3% MeOH as the eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495693B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-e5ac78d5040044b3903010c52c9a5766 |
| Source note | uspto-grants-2002_12 |