HuagongsheHuagongshe Chemistry Print Report · For research reference only
Adipic Acid → 1,4-Butanediol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Adipic Acid | HCID 196 | — |
| Reactant | Glutaric Acid | HCID 743 | — |
| Reactant | Succinic Acid | HCID 1110 | — |
| Product | 1,4-Butanediol | HCID 8064 | — |
| Product | 1,5-Pentanediol | HCID 8105 | — |
| Product | 1,6-Hexanediol | HCID 12374 | — |
Reaction Steps
The obtained reaction mixture was analyzed by HPLC and GC under the conditions mentioned above to determine the conversion of the starting material and the yield of the primary alcohol. The analysis showed that the conversions of succinic acid, glutaric acid and adipic acid were 93%, 93% and 97%, respectively, and the yields of 1,4-butanediol, 1,5-pentanediol and 1,6-hexanediol were 53%, 78% and 60%, respectively.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495730B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-3d918c64f14144ef8adc7eeaa6a34d60 |
| Source note | uspto-grants-2002_12 |