HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 11851001, compound → HCID 54000670, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 11851001 | HCID 11851001 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 54000670 | HCID 54000670 | 93.4% |
Reaction Steps
(4-Phenylethynyl-phenyl)-carbamic acid tert-butyl ester (Ih, 0.95 g, 3.24 mmol) was dissolved in MeOH (50 mL), treated with 20% Pd/C (0.1 g), and shaken under H2 (50 psi) for 22 hours. The reaction was filtered and concentrated to give 0.90 g (93%) of the desired product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06495715B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-b5481420f0ed4f3f907b4c1b3a6cc789 |
| Source note | uspto-grants-2002_12 |