Allyl bromide → HCID 67484939, compound

Participants

Reaction Steps

To a solution of 3-fluoro-4-nitrophenol (17.5 mmol, 2.75 g) and allyl bromide (17.5 mmol, 1.5 mL) in 10 mL of DMF was added K2CO3 (21 mmol, 2.9 g). The slurry was stirred at ambient temperature overnight, and partitioned into NaHCO3 (aq)/DCM. The organic phase was removed under reduced pressure affording the product as a brown oil. HPLC A: 2.19 min.

Provenance & Evidence