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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300133Generated: October 31, 2026

4-Methyloxybenzyl chloride → HCID 519849, compound

https://huagongshe.com/reaction/2300133

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-Methyloxybenzyl chlorideHCID 69993—
ReactantPhthalimide potassium saltHCID 24194345—
SolventDimethylformamideHCID 6228—
ProductHCID 519849HCID 51984990.8%

Reaction Conditions

Temperature50 °C

Reaction Steps

A mixture of 20 g 4-methoxybenzyl chloride, 26 g phthalimide potassium, and 100 ml dimethylformamide was stirred at 50° C. for 5 hr. After cooling, the reaction solution was poured into ice water and the resulting precipitates were collected by filtration. These were washed with water and dried to give 31 g of N-(4-methoxybenzyl)phthalimide.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498159B1
Source datasetuspto-grants-2002_12
ORD IDord-306e4d684f1845648fa7d6ea90efac2a
Source noteuspto-grants-2002_12