HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300133Generated: October 31, 2026
4-Methyloxybenzyl chloride → HCID 519849, compound
https://huagongshe.com/reaction/2300133
Participants
| Role | Name | HCID | Charge |
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| Reactant | 4-Methyloxybenzyl chloride | HCID 69993 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 519849 | HCID 519849 | 90.8% |
Reaction Steps
A mixture of 20 g 4-methoxybenzyl chloride, 26 g phthalimide potassium, and 100 ml dimethylformamide was stirred at 50° C. for 5 hr. After cooling, the reaction solution was poured into ice water and the resulting precipitates were collected by filtration. These were washed with water and dried to give 31 g of N-(4-methoxybenzyl)phthalimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06498159B1 |
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| Source dataset | uspto-grants-2002_12 |
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| ORD ID | ord-306e4d684f1845648fa7d6ea90efac2a |
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| Source note | uspto-grants-2002_12 |
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