HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperonylamine → HCID 43235900, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperonylamine | HCID 2723901 | — |
| Reactant | 2,1,3-Benzothiadiazole, 4-chlorosulfonyl- | HCID 2735459 | — |
| Product | HCID 43235900 | HCID 43235900 | — |
Reaction Steps
The title compound was prepared from benzo[1,2,5]thiadiazole-4-sulfonyl chloride and 4-piperidone monohydrate hydrochloride according to the procedure of Intermediate 22 as an off-white solid; 1H NMR (CDCl3) δ 2.57 (t, J=6.21 Hz, 2H), 3.77 (t, J=6.21 Hz, 2H), 7.60-7.84 (m, 1H), 8.25-8.32 (m, 1H), 8.40-8.46 (m, 1H); MS (ES) m/z 297.9 (MH+). C11H11N3O3S2
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498170B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-0fc03f6425b84021a17b59d085ffd2ce |
| Source note | uspto-grants-2002_12 |