HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53870459, compound → HCID 18376206, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53870459 | HCID 53870459 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 18376206 | HCID 18376206 | — |
Reaction Steps
The title compound was prepared following the method described in Example 1, Step C from 5-(3-{[3-(3-chloro-phenyl)-propyl]-cyclopropanesulfonyl-amino}-propyl)-thiophene-2-carboxylic acid methyl ester of Step A except the reaction was performed in EtOH. 1H NMR (400 MHz, CDCl3) δ 7.62 (d, 1H, J=3.4 Hz), 7.42-7.00 (m, 4H), 6.62 (d, 1H, J=3.4 Hz), 3.25 (m, 2H), 2.92 (m, 2H), 2.31 (m, 1H), 2.20 (m, 2H), 1.32-0.90 (m, 4H); MS 440 (M−1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498172B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-67fd25a7e3424ff5ad9507b65f1bdd5e |
| Source note | uspto-grants-2002_12 |