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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300446Generated: October 31, 2026

HCID 53870459, compound → HCID 18376206, compound

https://huagongshe.com/reaction/2300446

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 53870459HCID 53870459—
SolventEthanolHCID 702—
ProductHCID 18376206HCID 18376206—

Reaction Steps

The title compound was prepared following the method described in Example 1, Step C from 5-(3-{[3-(3-chloro-phenyl)-propyl]-cyclopropanesulfonyl-amino}-propyl)-thiophene-2-carboxylic acid methyl ester of Step A except the reaction was performed in EtOH. 1H NMR (400 MHz, CDCl3) δ 7.62 (d, 1H, J=3.4 Hz), 7.42-7.00 (m, 4H), 6.62 (d, 1H, J=3.4 Hz), 3.25 (m, 2H), 2.92 (m, 2H), 2.31 (m, 1H), 2.20 (m, 2H), 1.32-0.90 (m, 4H); MS 440 (M−1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498172B1
Source datasetuspto-grants-2002_12
ORD IDord-67fd25a7e3424ff5ad9507b65f1bdd5e
Source noteuspto-grants-2002_12