HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuryl chloride → HCID 54146619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuryl chloride | HCID 24648 | — |
| Reactant | 3-Fluorobenzenesulfonyl Chloride | HCID 2734258 | — |
| Reactant | {3-[(4-Thiazol-2-yl-benzylamino)-methyl]-phenoxy}-acetic Acid Tert-butyl Ester | HCID 53752425 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 54146619 | HCID 54146619 | — |
Reaction Steps
The title compound of Step A was prepared following the method described in Step A of Example 13w from {3-[(4-thiazol-2-yl-benzylamino)-methyl]-phenoxy}-acetic acid tert-butyl ester, prepared in Step A of Example 13i, and 3-fluorobenzenesulfonyl chloride with the following exception. The sulfonyl chloride was dissolved in CH2Cl2 (1 mL) and 0.28 mL was added to the reaction mixture. MS 569 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498172B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-e2ac3f62e3574cabab9fc424460f766e |
| Source note | uspto-grants-2002_12 |