HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-[3-(Benzenesulfonylamino-methyl)-phenyl]-propionic acid methyl ester → HCID 54262103, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-[3-(Benzenesulfonylamino-methyl)-phenyl]-propionic acid methyl ester | HCID 53970864 | — |
| Reactant | HCID 54321123 | HCID 54321123 | — |
| Product | HCID 54262103 | HCID 54262103 | — |
Reaction Steps
Following the procedure described in Step A of Example 2, 3-[3-(benzenesulfonylamino-methyl)-phenyl]-propionic acid methyl ester was alkylated with 1-(3-bromo-propenyl)-3,5-dichloro-benzene to provide the title compound of Step A. 1H NMR (400 MHz, CDCl3) δ 7.87 (dd, 2H), 7.63 (m, 1H), 7.55 (m, 2H), 7.22 (m, 2H), 7.07 (m, 3H), 6.93 (s, 2H), 6.11 (d, 1H), 5.77 (m, 1H), 4.34 (s, 2H), 3.87 (d, 2H), 3.66 (s, 3H), 2.87 (t, 2H), 2.54 (t, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498172B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-1cb38d0657c24403b57d611e93f1946c |
| Source note | uspto-grants-2002_12 |