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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300547Generated: October 29, 2026

3-[3-(Benzenesulfonylamino-methyl)-phenyl]-propionic acid methyl ester → HCID 54262103, compound

https://huagongshe.com/reaction/2300547

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-[3-(Benzenesulfonylamino-methyl)-phenyl]-propionic acid methyl esterHCID 53970864—
ReactantHCID 54321123HCID 54321123—
ProductHCID 54262103HCID 54262103—

Reaction Steps

Following the procedure described in Step A of Example 2, 3-[3-(benzenesulfonylamino-methyl)-phenyl]-propionic acid methyl ester was alkylated with 1-(3-bromo-propenyl)-3,5-dichloro-benzene to provide the title compound of Step A. 1H NMR (400 MHz, CDCl3) δ 7.87 (dd, 2H), 7.63 (m, 1H), 7.55 (m, 2H), 7.22 (m, 2H), 7.07 (m, 3H), 6.93 (s, 2H), 6.11 (d, 1H), 5.77 (m, 1H), 4.34 (s, 2H), 3.87 (d, 2H), 3.66 (s, 3H), 2.87 (t, 2H), 2.54 (t, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498172B1
Source datasetuspto-grants-2002_12
ORD IDord-1cb38d0657c24403b57d611e93f1946c
Source noteuspto-grants-2002_12