HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzamide → HCID 18376275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzamide | HCID 71572 | — |
| Reactant | Ethyl 3-bromo-2-oxopentanoate | HCID 14740334 | — |
| Product | HCID 18376275 | HCID 18376275 | — |
Reaction Steps
The title compound was prepared from 6.5 9 of 4-fluorobenzamide and 6.08 g of ethyl 3-bromo-2-oxo-pentanoate (as described in example 2B) to give 1.55 g (22%) of intermediate 3C as a solid: 1H NMR (CDCl3, 300 MHz) δ8.12-8.08 (m, 2H), 7.23-7.17 (m, 2H), 3.19 (q, 2H, J=7.5), 1.40 (t, 3H, J=7.5).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498174B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a22074afa27441939437663813211509 |
| Source note | uspto-grants-2002_12 |