HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methoxyphenethylamine → HCID 18375740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methoxyphenethylamine | HCID 74896 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 18375740 | HCID 18375740 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 2-(2-methoxyphenyl)ethylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 346.1 (M+1). 1H NMR (500 MHz, CDCl3): δ 8.66 (br s, 1H); 8.38 (br s, 1H); 8.22 (br s, 1H); 7.88 (d, J=6.7 Hz, 1H); 7.40 (m, 2H); 7.22 (m, 2H); 6.92 (m, 2H); 6.78 (d, J=5.4 Hz, 1H); 5.60 (br s, 1H); 3.88 (s, 3H); 3.78 (m, 2H); 3.03 (t, J=6.7 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-2d2d697c09904389b51b1fb0207e3efb |
| Source note | uspto-grants-2002_12 |