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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300728Generated: October 30, 2026

2-Methoxyphenethylamine → HCID 18375740, compound

https://huagongshe.com/reaction/2300728

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-MethoxyphenethylamineHCID 74896—
Reactant2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidineHCID 15549640—
ProductHCID 18375740HCID 18375740—

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 2-(2-methoxyphenyl)ethylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 346.1 (M+1). 1H NMR (500 MHz, CDCl3): δ 8.66 (br s, 1H); 8.38 (br s, 1H); 8.22 (br s, 1H); 7.88 (d, J=6.7 Hz, 1H); 7.40 (m, 2H); 7.22 (m, 2H); 6.92 (m, 2H); 6.78 (d, J=5.4 Hz, 1H); 5.60 (br s, 1H); 3.88 (s, 3H); 3.78 (m, 2H); 3.03 (t, J=6.7 Hz, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498165B1
Source datasetuspto-grants-2002_12
ORD IDord-2d2d697c09904389b51b1fb0207e3efb
Source noteuspto-grants-2002_12