HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzylamine → HCID 18375779, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzylamine | HCID 66035 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 18375779 | HCID 18375779 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 4-methylbenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 316.1 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.60 (s, 1H); 8.41 (br s, 1H); 8.09 (br s, 1H); 7.86 (m, 1H); 7.20 (d, J=8.0 Hz, 1H); 6.83 (d, J=5.3 Hz, 1H); 5.80 (br s, 1H); 4.71 (d, J=5.8 Hz, 2H); 2.37 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-48e8e8350fcb4459a55fc98abeb5b8b6 |
| Source note | uspto-grants-2002_12 |