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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300730Generated: October 31, 2026

4-Methylbenzylamine → HCID 18375779, compound

https://huagongshe.com/reaction/2300730

Reaction equation

Participants

RoleNameHCIDCharge
Reactant4-MethylbenzylamineHCID 66035—
Reactant2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidineHCID 15549640—
ProductHCID 18375779HCID 18375779—

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 4-methylbenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 316.1 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.60 (s, 1H); 8.41 (br s, 1H); 8.09 (br s, 1H); 7.86 (m, 1H); 7.20 (d, J=8.0 Hz, 1H); 6.83 (d, J=5.3 Hz, 1H); 5.80 (br s, 1H); 4.71 (d, J=5.8 Hz, 2H); 2.37 (s, 3H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498165B1
Source datasetuspto-grants-2002_12
ORD IDord-48e8e8350fcb4459a55fc98abeb5b8b6
Source noteuspto-grants-2002_12