HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Methylbenzylamine → HCID 18375464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Methylbenzylamine | HCID 6993 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 18375464 | HCID 18375464 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 2-methylbenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (CI): m/e 316.2 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.60 (s, 1H); 8.43 (br s, 1H); 8.05 (br s, 1H); 7.85 (d, J=8.7 Hz, 1H); 6.84 (d, J=5.4 Hz, 1H); 4.73 (d, J=5.7 Hz, 1H); 2.43 (s, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-faad647f7dca4128a3196115d1b5c52a |
| Source note | uspto-grants-2002_12 |