HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzylamine → HCID 18375656, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzylamine | HCID 66648 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 18375656 | HCID 18375656 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 2-chlorobenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (EI): m/e 335.0 (M+). 1H NMR (500 MHz, CDCl3): δ partial 8.60 (s, 1H); 8.43 (d, J=3.9 Hz, 1H); 8.02 (br s, 1H); 7.85 (m, 1H); 7.37 (m, 2H); 6.85 (d, J=5.5 Hz, 1H); 5.93 (br s, 1H); 4.85 (d, J=6.2 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-b61e90eaf68f4ac8850f5169b6cdaf7d |
| Source note | uspto-grants-2002_12 |