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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300744Generated: October 31, 2026

Benzenemethanamine, 3-chloro- → HCID 18375749, compound

https://huagongshe.com/reaction/2300744

Reaction equation

Participants

RoleNameHCIDCharge
ReactantBenzenemethanamine, 3-chloro-HCID 77802—
Reactant2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidineHCID 15549640—
ProductHCID 18375749HCID 18375749—

Reaction Steps

2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 3-chlorobenzylamine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (ESI): m/e 336.1 (M+1). 1H NMR (500 MHz, CDCl3): δ 8.58 (s, 1H); 8.45 (d, J=5.3 Hz, 1H); 8.01 (br s, 1H); 7.86 (m, 1H); 7.28 (m, 6H); 6.87 (d, J=5.3 Hz, 1H); 5.80 (br s, 1H); 4.74 (d, J=5.9 Hz, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06498165B1
Source datasetuspto-grants-2002_12
ORD IDord-dd4687c4e6544910bfe9847c9c05dfca
Source noteuspto-grants-2002_12