HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Pyridinemethanamine → HCID 18375809, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Pyridinemethanamine | HCID 77317 | — |
| Reactant | 2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine | HCID 15549640 | — |
| Product | HCID 18375809 | HCID 18375809 | — |
Reaction Steps
2-Methanesulfonyl-4-[benzimidazol-1-yl]pyrimidine was reacted with 4-(aminomethyl)pyridine according to the procedure described in EXAMPLE 1, Step C to afford the title compound. Mass Spectrum (CI): 303.1 (M+1). 1H NMR (500 MHz, CDCl3): δ partial 8.61 (d, J=5.8 Hz, 2H); 8.57 (br s, 1H); 8.44 (d, J=5.5 Hz, 1H); 7.85 (d, J=8.0 Hz, 1H); 6.89 (d, J=5.5 Hz, 1H); 5.96 (br s, 1H); 4.78 (d, J=6.4 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06498165B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-9e1ffce135554d34aaa71253de15cf2a |
| Source note | uspto-grants-2002_12 |