Azido(trimethyl)stannane → HCID 178461871, compound

Participants

Reaction Steps

2-[(S)-1-Phenylethylamino]-4-[5-cyanobenzimidazol-1-yl ]pyrimidine (20 mg) and trimethylstannylazide (18 mg) were heated (110° C.) in xylene for 15 hours. Upon cooling, the solution was evaporated to dryness and the residue was purified with preparatory thin-layer chromatography (SiO2, 5% MeOH/1% triethylamine in CH2Cl2) to yield 6 mg of the title compound Mass spectrum (ESI) 384.1 (M+1).

Provenance & Evidence