HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2300986Generated: November 2, 2026
Acetic Acid → Pyridine, 2-[[(2,5-dimethylphenyl)methyl]sulfonyl]-6-methyl-, 1-oxide
https://huagongshe.com/reaction/2300986
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Hydrogen Peroxide | HCID 784 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | HCID 18377467 | HCID 18377467 | — |
| Catalyst | Sodium tungstate | HCID 26052 | — |
| Product | Pyridine, 2-[[(2,5-dimethylphenyl)methyl]sulfonyl]-6-methyl-, 1-oxide | HCID 501186 | — |
Reaction Steps
The sulfide isolated in step (a) above was dissolved in 15 ml of glacial acetic acid and then 2 ml of 30% hydrogen peroxide was added along with 50 mg of sodium tungstate. The reaction mixture was heated at 40° C. for two hours, cooled, and poured into water to percipitate the product. Yield, 1.53 g.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US06498254B1 |
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| Source dataset | uspto-grants-2002_12 |
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| ORD ID | ord-ca3f29a70baa45e490a60d61ef56fa7c |
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| Source note | uspto-grants-2002_12 |
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