2-Amino-1-naphthol → HCID 22764064, compound

HRID 230104Notes

Reaction equation

HRID 230104 reaction equation
[NH2:1][C:2]1[CH:11]=[CH:10][C:9]2[C:4](=[CH:5][CH:6]=[CH:7][CH:8]=2)[C:3]=1[OH:12].[Cl:13][CH2:14][C:15](OCC)(OCC)OCC>C(O)C>[Cl:13][CH2:14][C:15]1[O:12][C:3]2[C:4]3[C:9](=[CH:8][CH:7]=[CH:6][CH:5]=3)[CH:10]=[CH:11][C:2]=2[N:1]=1

Participants

4

Reactant 2

HCID 390382-Amino-1-naphtholHCID 3059222-Chloro-1,1,1-triethoxyethane

Product 1

HCID 22764064HCID 22764064, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Prepared by reacting 2.93 g of 2-amino-1-naphthol with 3.54 g of 2-chloro-1,1,1-triethoxy-ethane in 25 ml of ethanol at 60° C.

Workup

  1. customPrepared
  2. customat 60° C.

Sources & evidence

ORD record
ord-4751dfa9607a49c19238d93a800c6d82
Source dataset
uspto-grants-2009_07
Patent number
US07566707B2

Reaction notes

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