HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 11647391, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | Chlorophenyl isocyanate | HCID 76833 | — |
| Reactant | HCID 18373545 | HCID 18373545 | — |
| Product | HCID 11647391 | HCID 11647391 | 32% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, N-isopropyl-3-amino-6-chloro-2-hydroxybenzenesulfonamide (220 mg, 0.88 mmol) and 2-chlorophenylisocyanate (135 mg, 0.88 mmol) were coupled to form the desired urea (110 mg, 32%). EI-MS m/z417.1 (M-H)−.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-a7a1b2ca854e43459b4d68b37fdddf60 |
| Source note | uspto-grants-2002_12 |