HuagongsheHuagongshe Chemistry Print Report · For research reference only
Bromhydrol → HCID 11511649, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Bromhydrol | HCID 166749 | — |
| Reactant | HCID 11613392 | HCID 11613392 | — |
| Product | HCID 11511649 | HCID 11511649 | 14.3% |
Reaction Steps
Following the deprotection procedure outlined in example 58, N-[4-chloro-3-[N″,N″-di-(2-methoxyethyl)aminosulfonyl]-2-hydroxyphenyl]-N′(2,3-dichlorophenyl) urea (15 mg, 0.028 mmol) and aluminum bromide (18.7 mg, 0.07 mmol) were reacted to give the desired product (2 mg, 14%). LC-MS 500.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-2509ecaf4a714c1bb48908d561bfd18c |
| Source note | uspto-grants-2002_12 |