HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 54136846, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | Chlorophenyl isocyanate | HCID 76833 | — |
| Reactant | HCID 18373537 | HCID 18373537 | — |
| Product | HCID 54136846 | HCID 54136846 | 43.3% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, 4-chloro-2-hydroxy-3-(1-oxidothiomorpholinosulfonyl)aniline (117 mg, 0.35 mmol) and 2-chlorophenylisocyanate (58 mg, 0.28mmol) were coupled to form the desired urea (58 mg, 35%). LC-MS (m/z) 478.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-cff47732b2b24a99acc2acc751e5b8db |
| Source note | uspto-grants-2002_12 |