HuagongsheHuagongshe Chemistry Print Report · For research reference only
Urea → HCID 11676032, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Urea | HCID 1176 | — |
| Reactant | 1,2-Dichloro-3-isocyanatobenzene | HCID 33050 | — |
| Reactant | HCID 18373528 | HCID 18373528 | — |
| Product | HCID 11676032 | HCID 11676032 | 42.7% |
Reaction Steps
Following the general procedure for urea formation outlined in example 15, 3-(azetidin-1-yl)sulfonyl-4-chloro-2-hydroxyaniline (235 mg, 0.9 mmol) and 2,3-dichlorophenylisocyanate (169 mg, 0.9 mmol) were coupled to form the desired urea (160 mg, 40%). LC-MS 450.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-ea72e9621f8d42878e399ea1c6c46edf |
| Source note | uspto-grants-2002_12 |