HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 86588376, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 86587417 | HCID 86587417 | — |
| Product | HCID 86588376 | HCID 86588376 | 77% |
Reaction Steps
Following the general hydrolysis procedure outlined in example 15, (N-isoxazolidinyl)-2,6-dichloro-3-nitrobenzenesulfonamide (1.08 g, 3.3 mmol), 80% NaH (0.3 g, m10.0 mol) and water (72 μL, 4 mmol) were reacted to form the desired product (0.79 g, 77%). LC-MS m/z 309(M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-b1dfe6d9fc3446b2a7aa7cc2190ca9f7 |
| Source note | uspto-grants-2002_12 |