HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53927156, compound → HCID 69824964, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53927156 | HCID 53927156 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 69824964 | HCID 69824964 | 139% |
Reaction Steps
Following the general procedure for Boc deprotection in example 36, N-[3-[N″-[5-(tert-butoxycarbonylamino)-5-carboxypentyl]aminosulfonyl]-4-chloro-2-hydroxyphenyl]-N′(2-chlorophenyl) urea (104 mg, 0.17 mmol) was stirred in 1 mL of trifluoroacetic acid to form the desired product (64 mg, 61%). LC-MS (m/z) 505.0 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500863B1 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-b4d2956e9818435abc536a656d190865 |
| Source note | uspto-grants-2002_12 |