Sodium hydrosulfide → HCID 178509032, compound

HRID 2301678Notes

Reaction equation

HRID 2301678 reaction equation
[NH2:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[C@@H:11]2[O:17][C@H:16]([CH2:18][OH:19])[C@H:14]([OH:15])[C@H:12]2[OH:13])=[C:4](Cl)[N:3]=1.[SH-:21].[Na+]>>[NH2:1][C:2]1[N:10]=[C:9]2[C:5]([N:6]=[CH:7][N:8]2[C@@H:11]2[O:17][C@H:16]([CH2:18][OH:19])[C@H:14]([OH:15])[C@H:12]2[OH:13])=[C:4]([SH:21])[N:3]=1

Participants

3

Reactant 2

HCID 28015Sodium hydrosulfideHCID 142841022-amino-6-chloro-9-(beta-D-xylofuranosyl)purine

Product 1

HCID 178509032HCID 178509032, compound

Procedure

2-Amino-6-chloro-9-(β-D-xylofuranosyl)purine as prepared by the Example 6, Method B, is treated with sodium hydrosulfide to give the title compound.

Sources & evidence

ORD record
ord-d89d321c4dd14e70af07706282896e16
Source dataset
uspto-grants-2002_12
Patent number
US06500945B2

Reaction notes

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