HuagongsheHuagongshe Chemistry Print Report · For research reference only
1H-indole-6-carboxylic acid → 4-t-Butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-N1-(6-indolylcarbonyl)-1,2-benzenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1H-indole-6-carboxylic acid | HCID 595230 | — |
| Reactant | 4-t-butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-1,2-benzenediamine | HCID 11795190 | — |
| Product | 4-t-Butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-N1-(6-indolylcarbonyl)-1,2-benzenediamine | HCID 53784454 | 50% |
Reaction Steps
Using the procedure described in Example 9, Part C, 4-t-butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-1,2-benzenediamine (1.15 g, 2.9 mmol) and indole-6-carboxylic acid (0.46 g, 2.9 mmol) yielded 780 mg (50%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500851B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-17c0900a270d480487753edf52287334 |
| Source note | uspto-grants-2002_12 |