HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-t-butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-1,2-benzenediamine → 4-t-Butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-N1-(3-bromoindol-6-ylcarbonyl)-1,2-benzenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-t-butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-1,2-benzenediamine | HCID 11795190 | — |
| Reactant | 3-Bromo-1H-indole-6-carboxylic acid | HCID 15543043 | — |
| Product | 4-t-Butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-N1-(3-bromoindol-6-ylcarbonyl)-1,2-benzenediamine | HCID 53739518 | 79% |
Reaction Steps
Using the procedure described in Example 9, Part C, 4-t-butyldimethylsilyloxy-N2-(4-t-butylbenzoyl)-1,2-benzenediamine (750 mg, 1.9 mmol) and 3-bromoindole-6-carboxylic acid (456 mg, 1.9 mmol) yielded 930 mg (79%) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06500851B2 |
| Source dataset | uspto-grants-2002_12 |
| ORD ID | ord-4d957149532942c1acc5bc442eeef421 |
| Source note | uspto-grants-2002_12 |