2-Oxobutanoic Acid → HCID 86758390, compound

HRID 2301959Notes

Reaction equation

HRID 2301959 reaction equation
[NH2:1][C@H:2]([C:8]([OH:10])=[O:9])[CH2:3][CH2:4][CH2:5][CH2:6][NH2:7].[O:11]=[C:12]([CH2:16][CH3:17])[C:13]([OH:15])=[O:14].CC(C)=O>CO>[O:11]=[C:12]([CH2:16][CH3:17])[C:13]([OH:15])=[O:14].[NH2:1][C@H:2]([C:8]([OH:10])=[O:9])[CH2:3][CH2:4][CH2:5][CH2:6][NH2:7]

Participants

5

Reactant 3

HCID 582-Oxobutanoic AcidHCID 180AcetoneHCID 5962L-Lysine

Product 1

HCID 86758390HCID 86758390, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

Lysine (1.46 g; 10 mmoles) and oxobutyric acid (1.02 g; 10 mmoles) are dissolved in 5 ml of methanol. Acetone is added, and the precipitate filtered out.

Workup

  1. filtrationthe precipitate filtered out

Sources & evidence

ORD record
ord-1f6891544dca452ca57b80afae2f52b6
Source dataset
uspto-grants-2002_08
Patent number
US06429229B1

Reaction notes

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