Pyridine → HCID 8317679, compound

HRID 2302043Notes

Reaction equation

HRID 2302043 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=[CH:3][C:2]=1[C:11](Cl)=[O:12].[CH:14]1([NH2:21])[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]1.N1C=CC=CC=1>O>[CH:14]1([NH:21][C:11]([C:2]2[CH:3]=[N:4][C:5]3[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=3)[N:1]=2)=[O:12])[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15]1

Participants

5

Reactant 3

HCID 1049PyridineHCID 2899CycloheptylamineHCID 2734681Quinoxaline-2-carbonyl chloride

Product 1

HCID 8317679HCID 8317679, compoundYield 12.4%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Prepared from 2-quinoxaloyl chloride (193 mg, 1.0 mmol), cycloheptylamine (115 μL, 102 mg, 0.90 mmol), pyridine (5 mL), and water (100 mL) yielding 30 mg (12%) of (229):

Sources & evidence

ORD record
ord-09ca32cada414243acb672685dfcfd83
Source dataset
uspto-grants-2002_08
Patent number
US06429207B1

Reaction notes

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