2,3-Dimethylcyclohexylamine → HCID 22136401, compound

HRID 2302052Notes

Reaction equation

HRID 2302052 reaction equation
[N:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[N:4]=[CH:3][C:2]=1[C:11](Cl)=[O:12].[CH3:14][CH:15]1[CH:20]([CH3:21])[CH2:19][CH2:18][CH2:17][CH:16]1[NH2:22]>N1C=CC=CC=1>[CH3:14][CH:15]1[CH:20]([CH3:21])[CH2:19][CH2:18][CH2:17][CH:16]1[NH:22][C:11]([C:2]1[CH:3]=[N:4][C:5]2[C:10](=[CH:9][CH:8]=[CH:7][CH:6]=2)[N:1]=1)=[O:12]

Participants

4

Reactant 2

HCID 1235072,3-DimethylcyclohexylamineHCID 2734681Quinoxaline-2-carbonyl chloride

Product 1

HCID 22136401HCID 22136401, compoundYield 59%

Reagents, catalysts & solvents 1

HCID 1049PyridineSolvent

Procedure

Prepared from 2-quinoxaloyl chloride (193 mg, 1.0 mmol), 2,3-dimethylcyclohexylamine (115 mg, 0.90 mmol), and pyridine (5 mL) yielding 150 mg (59%) of (163):

Sources & evidence

ORD record
ord-71f814d73ac34caa9f8a1c83516aaff8
Source dataset
uspto-grants-2002_08
Patent number
US06429207B1

Reaction notes

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