HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(4-Methoxyphenyl)-1,1-dimethylethylamine → HCID 18459605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(4-Methoxyphenyl)-1,1-dimethylethylamine | HCID 91892 | — |
| Reactant | 2-(3-Chlorophenoxymethyl)oxirane | HCID 9899028 | — |
| Product | HCID 18459605 | HCID 18459605 | 83.9% |
Reaction Steps
Using the method of Example 25, supra, 3-chlorophenyl glycidyl ether (1.0 mmol) and 1,1-dimethyl-2-(4-methoxyphenyl)ethylamine (1.25 mmol) yielded 168 mg of the title compound as a white solid: GC/EI-MS, m/z (rel. int.) 348 (M−15, 0.9), 245 (7), 244 (35), 243 (25), 242 (100), 163 (7), 121 (22), 71 (11), 70 (16).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432656B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-766ae7b7fd7044999dea2166fa75a706 |
| Source note | uspto-grants-2002_08 |