HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chlorphentermine → HCID 22640794, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chlorphentermine | HCID 10007 | — |
| Reactant | Phenyl glycidyl ether | HCID 31217 | — |
| Product | HCID 22640794 | HCID 22640794 | 10.3% |
Reaction Steps
Using the method of Example 6, supra, 1,2-epoxy-3-phenoxypropane (950 mg, 6.3 mmol) and 1,1-dimethyl-2-(4-chlorophenyl)ethylamine (1.45 g, 7.9 mmol) were used to prepare 150 mg of the title compound as a white solid: GC/EI-MS, m/z (rel. int.) 318 (M−15, 7), 209 (47), 208 (100), 127 (11), 125 (33), 114 (13), 107 (12), 77 (23), 71 (16), 70 (29), 58 (13).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06432656B1 |
| Source dataset | uspto-grants-2002_08 |
| ORD ID | ord-a6560fe695bd4000983802e5f9b1ad47 |
| Source note | uspto-grants-2002_08 |