6-Methoxy-2-(4-methoxyphenyl)benzo[b]thiophene → HCID 18461170, compound

HRID 2303384Notes

Reaction equation

HRID 2303384 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[S:13][C:12]3[CH:14]=[C:15]([O:18][CH3:19])[CH:16]=[CH:17][C:11]=3[CH:10]=2)=[CH:5][CH:4]=1.[N:20]1([CH2:26][CH2:27][O:28][C:29]2[C:37]([CH3:38])=[CH:36][C:32]([C:33](O)=[O:34])=[CH:31][C:30]=2[CH3:39])[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]1>>[CH3:1][O:2][C:3]1[CH:8]=[CH:7][C:6]([C:9]2[S:13][C:12]3[CH:14]=[C:15]([O:18][CH3:19])[CH:16]=[CH:17][C:11]=3[C:10]=2[C:33]([C:32]2[CH:36]=[C:37]([CH3:38])[C:29]([O:28][CH2:27][CH2:26][N:20]3[CH2:25][CH2:24][CH2:23][CH2:22][CH2:21]3)=[C:30]([CH3:39])[CH:31]=2)=[O:34])=[CH:5][CH:4]=1

Participants

3

Reactant 2

HCID 8509416-Methoxy-2-(4-methoxyphenyl)benzo[b]thiopheneHCID 18461150HCID 18461150, compound

Product 1

HCID 18461170HCID 18461170, compound

Procedure

2.9 g of the title compound was prepared from 2 g of 2-(4-methoxyphenyl)-6-methoxybenzo[b]thiophene and 4-[2-(1-piperidinyl)ethoxy]-3,5,-dimethylbenzoic acid in a manner similar to that used in Preparation 15.

Workup

  1. customthat used in Preparation 15

Sources & evidence

ORD record
ord-1474e08abd3e423ba89445b98639e7cc
Source dataset
uspto-grants-2002_08
Patent number
US06432982B1

Reaction notes

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