Ammonia → HCID 18461541, compound

Participants

Reaction Steps

Analogously to the procedures of Example 1, the title compound was prepared from 0.31 g (2.5 mmol) of 3,3a,4,6a-tetrahydro-cyclopenta[b]furan-2-one, 2.5 ml of a 1 molar lithium bis-(trimethylsilyl)-amide solution in THF and 0.36 g (2.5 mmol) of allyl bromide in 7 ml of THF. Yield: 278 mg (67.8%) of a colourless oil. MS (DCI/NH3): m/e=182 [M+NH4+]

Provenance & Evidence