Cyclohexylhydroxylamine → HCID 86587894, compound

HRID 2303532Notes

Reaction equation

HRID 2303532 reaction equation
[CH2:1]([O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=O)=[CH:11][C:10]=1[O:17][CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH:19]1([NH:25][OH:26])[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]1>>[CH2:1]([O:8][C:9]1[CH:16]=[CH:15][C:12]([CH:13]=[N+:25]([CH:19]2[CH2:24][CH2:23][CH2:22][CH2:21][CH2:20]2)[O-:26])=[CH:11][C:10]=1[O:17][CH3:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1

Participants

3

Reactant 2

HCID 72935CyclohexylhydroxylamineHCID 755064-(Benzyloxy)-3-methoxybenzaldehyde

Product 1

HCID 86587894HCID 86587894, compound

Procedure

The title compound was prepared according to the procedure described in Example 11 using 4-benzyloxy-3-methoxybenzaldehyde and N-cyclohexylhydroxylamine. The title compound was isolated in 97.9% yield as a solid, m.p. 154.1° C.

Workup

  1. customThe title compound was prepared

Sources & evidence

ORD record
ord-58aa6581ecc941beb7d2750157b886cd
Source dataset
uspto-grants-2002_08
Patent number
US06433008B1

Reaction notes

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